閲嶅簡縐戞亽鏈虹數(shù)璁懼鏈夐檺鍏徃涓烘?zhèn)ㄥ厤璐规彁渚涢噸搴嗗簾姘斿鐞嗐�侀噸搴嗚濺闂村簾姘旀不鐞嗗摢瀹跺ソ銆侀噸搴嗗簾鏃х數(shù)鐡跺洖鏀朵環(huán)鏍肩瓑鐩稿叧淇℃伅鍙戝竷鍜岃祫璁紝鏁鍏蟲敞錛?/div>
鎮(zhèn)ㄥ綋鍓嶇殑浣嶇疆錛?a href="/">棣栭〉 > 琛屼笟鍔ㄦ�?/a> > 璇︾粏鍐呭
鍦熷￥涓尌鍙戞�ф湁鏈虹墿嫻嬪畾鐮旂┒
鍙戝竷鏃ユ湡錛?021-03-16
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嫻嬪畾鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勭浉鍏沖唴瀹癸紝瀵規(guī)尌鍙戞�ф湁鏈虹墿榪涜姒傝堪闈炲父閲嶈錛屽彲浠ユ竻妤氬湡澹ゆ尌鍙戞�ф湁鏈虹墿姹℃煋鐨勭壒寰佷笌鐗圭偣錛岄�夋嫨鎭板綋鐨勫湡澹ゆ尌鍙戞�ф湁鏈虹墿嫻嬪畾鏂規(guī)硶錛岄�氳繃瀹為獙鎵嬫錛岃繘琛屽疄楠屽垎鏋愶紝瀵圭粨鏋滆繘琛屾繁鍏ョ殑璁ㄨ鎺㈢┒錛屼繚璇佸伐浣滅殑欏哄埄瀹炴柦銆傜敱姝ゅ彲瑙侊紝鐮旂┒鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氬叿鏈夐噸瑕佺殑鎰忎箟涓庝環(huán)鍊鹼紝鏈夊姪浜庡彂鎸ラ噸瑕佺殑浣滅敤錛屾帉鎻℃湁鏁堢殑鍦熷￥鎸ュ彂鎬ф湁鏈虹墿嫻嬪畾鏂規(guī)硶錛屼繚璇佹祴瀹氱殑縐戝鎬т笌鍚堢悊鎬с�?/span>
涓�銆佹尌鍙戞�ф湁鏈虹墿鐨勬榪?/span>
闅忕潃縐戞妧鐨勫揩閫熷彂灞曪紝鐜頒唬鍐滀笟鍜屽寲宸ヤ紒涓氭帓鏀句簡澶ч噺搴熸按銆佸簾姘斻�佸簾鐗╋紝鍦ㄥ湡澹ゃ�佺┖姘斾互鍙婄敓鐗╃瓑浠嬭川鐨勮漿鍖栦笅錛岄暱鏈熷瓨鍦ㄤ簬鍦熷￥浠ュ強姘翠綋涓紝褰㈡垚鍥哄畾姹℃煋[1]銆傛綾葷墿璐ㄤ笌浜洪暱鏈熸帴瑙︼紝鏋佹槗閫犳垚浜轟綋鎱㈡�т腑姣掞紝鐢氳嚦浼?xì)璇卞彂鐧岀棁锛屽錆h綾婚�犳垚杈冨ぇ鐨勫獎鍝嶏紝鐩存帴褰卞搷鍒扮敓孌栦笌涓灑紲炵粡緋葷粺錛屽湪涓ラ噸鎯呭喌涓嬶紝鐢氳嚦浼?xì)瀵艰嚧錆h綾繪浜★紝鍚屾椂錛屼篃浼?xì)瀵圭幆澧冨甫鏉ヤ弗閲嶇殑鍗卞疅雬傞櫎姝や箣澶栵紝搴熺墿緇忚繃闆ㄦ按鐨勫啿鍒鳳紝浼?xì)瀵瑰湴琛ㄦ按浠ュ強鍦颁笅姘撮�犳垚姹℃煋錛屽鑷翠弗閲嶇殑鍚庢灉銆傚熀浜庢錛岀爺絀跺湡澹や腑鎸ュ彂鎬ф湁鏈虹墿媯�嫻嬮潪甯擱噸瑕侊紝涓嬮潰瀵規(guī)尌鍙戞�ф湁鏈虹墿榪涜璇︾粏鐨勬榪般�傜幇闃舵錛屾尌鍙戞�ф湁鏈虹墿鐨勬潵婧愪富瑕佸垎涓轟互涓嬩袱縐嶏紝浜轟負(fù)鎺掓斁鐨勪笌鑷劧鎺掓斁鐨勩�備漢涓烘帓鏀劇殑涓昏鍖呮嫭鍖栧伐鐢熶駭浜х敓鐨勬苯杞﹀熬姘斻�傛尌鍙戞�ф湁鏈虹墿瀵逛漢浣撳拰鐜鏈夌潃杈冨ぇ鐨勫嵄瀹籌紝鍥犳錛屼漢綾誨湪闀挎湡鍙楀埌鎸ュ彂鎬ф湁鏈虹墿鍗卞鏃訛紝鏋佹槗浜х敓鐥呭彉錛屽獎鍝嶄漢綾昏韓浣撳仴搴楓�傛尌鍙戞�ф湁鏈虹墿涓昏鏉ヨ嚜瀹ゅ錛屽澶栦富瑕佹槸鐢變簬鐕冩枡浠ュ強宸ヤ笟搴熸皵銆佹苯杞﹀熬姘旂瓑璇卞彂鐨勩�傚嚭鐜版尌鍙戞�ф湁鏈虹墿鐨勫師鍥犱富瑕佹槸澶╃劧姘旂噧鐑с�佸惛鐑熴�佺児璋冧互鍙婇噰鏆栥�傚湪瀹ゅ唴瑁呴グ榪囩▼涓紝鎸ュ彂鎬ф湁鏈虹墿鍒欎富瑕佹潵鑷簬娑傛枡浠ュ強娌規(guī)紗銆傛尌鍙戞�ф湁鏈虹墿浣滀負(fù)涓�縐嶆薄鏌撴簮錛屼富瑕佸垎涓轟互涓嬪嚑縐嶏細(xì)涓�錛屾湁鏈烘憾娑層�傛湁鏈烘憾娑蹭富瑕佹槸鐢辨湁鏈虹墿緇勬垚鐨勬憾鍓傦紝鍏朵腑鐨勬樉钁椾唬琛ㄥ氨鏄寲濡嗗搧銆佹補婕嗐�佺矘鍚堝墏浠ュ強鍚按娑傛枡絳夛紱浜岋紝寤虹瓚鏉愭枡錛屽緩絳戞潗鏂欐槸鎸囧緩絳戝伐紼嬩腑浣跨敤鐨勬尌鍙戞皵鍛蟲潗鏂欙紝涓昏鍖呮嫭浜洪�犳澘鏉愩�佹秱鏂欍�佹場娌殧鐑潗鏂欑瓑[2]錛涗笁錛岀氦緇存潗鏂欙紝綰ょ淮鏉愭枡鏄寚鍚堟垚綰ょ淮鍒舵垚鐨勬潗鏂欎互鍙婂ぉ鐒剁氦緇村埗鎴愮殑鏉愭枡錛屼富瑕佹寚鍦版銆佸寲綰ょ獥甯樹互鍙婃寕姣瓑錛涘洓錛屽澶栧伐涓氭皵浣擄紝瀹ゅ宸ヤ笟姘斾綋鑼冨洿騫挎硾錛屼富瑕佹槸鎸囧伐涓氱敓浜т互鍙婃満姊版暎鍙戝嚭鏉ョ殑姘斾綋銆佺敓浜ц繃紼嬪埗閫犵殑浠ュ強姹借濺灝炬皵絳夈�?/span>
浜屻�佸湡澹ゆ尌鍙戞�ф湁鏈虹墿姹℃煋鐨勭壒鎬т笌鐗瑰緛
鎸ュ彂鎬ф湁鏈虹墿浣滀負(fù)涓�縐嶆薄鏌撴簮錛屽叿鏈夋樉钁楃殑姹℃煋鐗規(guī)�э紝鍏舵薄鏌撶壒鎬т笌鐗瑰緛涓昏浣撶幇鍦ㄤ互涓嬩袱涓柟闈紝鍒嗗埆鏄尌鍙戞�ф湁鏈虹墿鐨勬薄鏌撶壒鎬т互鍙婂湪鍦熷￥涓殑鍒嗗竷榪佺Щ銆?/span>
鎸ュ彂鎬ф湁鏈虹墿鐨勬薄鏌撶壒鎬т富瑕佸寘鎷互涓嬪洓涓柟闈㈠唴瀹癸細(xì)涓�錛屾尌鍙戞�э紝鎸ュ彂鎬ф湁鏈虹墿鐨勬樉钁楃壒寰佸氨鏄叿鏈夎緝寮虹殑鎸ュ彂鎬э紝涓�鏃︽弧瓚沖帇鍔涗笌娓╁害鏉′歡錛屽氨鑳藉浠庡湡澹や腑鎸ュ彂錛屽茍榪涘叆澶ф皵錛岄�犳垚涓ラ噸鐨勫嵄瀹籌紝鍏鋒湁杈冨己鐨勬薄鏌撴�э紱浜岋紝闅愯斀鎬э紝鍦熷￥涓殑鎸ュ彂鎬ф湁鏈虹墿鍏鋒湁杈冨己鐨勯殣钄芥�э紝甯稿父浼?xì)闅愯棌鍦ㄥ湡澹や腑锛寴q樹細(xì)闅愯棌鍦ㄦ皵浣撱�佹恫浣撱�佸浐浣撶瓑鐗╄川涓紝鍏鋒湁闈炲父澶х殑闅愯棌鎬э紱涓夛紝鎸佷箙鎬э紝鎸ュ彂鎬ф湁鏈虹墿涓�鏃﹁繘鍏ュ埌澶ф皵涓紝鏄壒鍒毦浠ユ竻闄ょ殑錛岄殢鐫�鎸ュ彂閲忕殑鎻愬崌錛屾祿搴︾殑涓嶆柇鎻愰珮錛屽叾緇撴灉鏄祿搴︿細(xì)瓚呰繃浜轟綋鐨勫彲鎵垮彈鑼冨洿錛屽浜轟綋閫犳垚涓嶅彲鎸藉洖鐨勪激瀹籌紝鍗卞浜轟綋鐨勮韓浣撳仴搴鳳紱鍥涳紝姣掑鎬э紝鎸ュ彂鎬ф湁鏈虹墿澶у鏄叿鏈夋瘨鎬х殑錛屼笖姣掓�ц緝寮猴紝灝ゅ叾鏄湁姣掓�х殑姹℃煋鐗╂尌鍙戝埌澶ф皵涓紝浼?xì)迮炴垚鍏夊寲瀛︾儫闆惧Q屽澶ф皵鐜閫犳垚涓ラ噸鐨勫獎鍝嶃�?/span>
鎸ュ彂鎬ф湁鏈虹墿鍦ㄥ湡澹や腑鐨勮縼縐葷壒鎬э紝浠ユ皵鎬佷互鍙婃恫鎬佷袱縐嶆柟寮忓嚭鐜幫紝鍐嶈�咃紝鎸ュ彂鎬ф湁鏈虹墿鍏鋒湁寮虹儓鐨勬尌鍙戞�э紝瀹規(guī)槗榪涘叆鍒頒漢綾葷敓媧葷殑澶ф皵涓紝涔熷鏄撹繘鍏ュ埌姘翠腑錛屾瀬鏄撳浜虹被鐢熸椿閫犳垚濞佽儊銆傚悓鏃訛紝鎸ュ彂鎬ф湁鏈虹墿涔熷叿澶囪縼縐繪�э紝淇濊瘉鍏跺緇堝浜庡姩鎬佸彉鍖栬繃紼嬩腑錛屼笖鏄笉鏂彉鍖栫殑錛屽洜鑰岋紝鎸ュ彂涔熸槸涓�縐嶈縼縐葷殑鏂瑰紡錛屽叿鏈夎縼縐葷壒鎬с�?/span>
涓夈�佸湡澹や腑鎸ュ彂鎬ф湁鏈虹墿嫻嬪畾鏂規(guī)硶
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涓�錛屼究鎼哄紡姘旂浉鑹茶氨浠硶[2]銆備究鎼哄紡姘旂浉鑹茶氨浠槸涓�嬈捐秴鐏墊晱銆佷綆鍔熻�楀拰蹇�熸嫻嬫尌鍙戞�ф湁鏈虹墿鐨勪究鎼哄紡姘旂浉鑹茶氨浠紝灝ゅ叾閫傜敤浜庢嫻嬫尌鍙戞�ф湁鏈虹墿濡傝嫰銆佺敳鑻�佷箼鑻�侀偦錛岄棿錛屽浜岀敳鑻瓑鑻郴鐗╋紝鐗圭偣浣撶Н灝忋�侀噸閲忚交錛屽叿鏈夎秴楂樼伒鏁忓害鐨勫厜紱誨瓙鍖栨嫻嬪櫒銆備富瑕佹槸瀵圭┖姘斿唴鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氥�?/span>
浜岋紝鍚規(guī)壂鎹曢泦娉曘�傚惞鎵崟闆嗘妧鏈�傜敤浜庝粠娑蹭綋鎴栧浐浣撴牱鍝佷腑钀冨彇娌哥偣浣庝簬200鈩冦�佹憾瑙ｅ害灝忎簬2%鐨勬尌鍙戞�ф垨鍗婃尌鍙戞�ф湁鏈虹墿錛屾槸鐜鐩戞祴涓噸瑕佺殑鏂規(guī)硶銆傚湪娑蹭綋鎴栧浐浣撲腑鐨勬尌鍙戞�ф湁鏈虹墿錛岀敤姘皵銆佹唉姘旀垨鍏跺畠鎯版�ф皵浣撳皢琚祴鐗╀粠鏍峰搧涓娊鎻愬嚭鏉ャ�傚惞鎵崟闆嗘妧鏈嬌姘斾綋榪炵畫閫氳繃鏍峰搧錛屽皢鍏朵腑鐨勬尌鍙戠粍鍒嗚悆鍙栧悗鍦ㄥ惛闄勫墏鎴栧喎闃變腑鎹曢泦錛屽啀榪涜鍒嗘瀽嫻嬪畾錛屾槸涓�縐嶉潪騫寵 鎬佺殑榪炵畫钀冨彇銆傚惞鎵崟闆嗘硶瀵規(guī)牱鍝佺殑鍓嶅鐞嗘棤闇�浣跨敤鏈夋満婧跺墏錛屽鐜涓嶉�犳垚浜屾姹℃煋錛岃�屼笖鍏鋒湁鍙栨牱閲忓皯銆佸瘜闆嗘晥鐜囬珮銆?/span>
鍦ㄥ惞鎵崟闆嗘硶搴旂敤榪囩▼涓紝褰卞搷嫻嬭瘯緇撴灉鐨勫師鍥犱富瑕佹湁涓や釜鏂歸潰錛屼竴鏄惞鎵椂闂寸殑閫夋嫨錛屽惞鎵椂闂存槸褰卞搷鐏墊晱搴︿互鍙婂洖鏀剁巼鐨勯噸瑕佸洜绱狅紝鍦ㄥ惞鎵椂闂磋緝闀跨殑鎯呭喌涓嬶紝浼?xì)鍚硅劚鍚搁檮鍓傚Q屽獎鍝嶆祴瀹氭晥鏋溿�傚湪鍚規(guī)壂鏃墮棿鍋忕煭鐨勬儏鍐典笅錛屽垎鏋愮墿鎸ュ彂涓嶅厖鍒嗭紝涔熶細(xì)褰卞搷嫻嬪畾鏁堟灉銆備簩鏄敳閱囦笌姘寸殑騫叉壈銆傚湪鍚規(guī)壂鎹曢泦娉曞簲鐢ㄨ繃紼嬩腑錛岀敳閱囦笌姘翠細(xì)瀵規(guī)祴瀹氭晥鏋滈�犳垚褰卞搷錛屽共鎵版嫻嬪櫒淇″彿錛屽獎鍝嶆嫻嬬殑鍑嗙‘搴3]銆?/span>
涓夛紝鍥虹浉寰悆鍙栵紙SPME錛夊浐鐩稿井钀冨彇鎶�鏈紙SPEM錛夋槸榪戝勾鏉ュ彂灞曡搗鏉ヤ竴縐嶆棤闇�婧跺墏錛岄泦钀冨彇銆佹祿緙╁拰榪涙牱涓轟竴浣撶殑鏍峰搧鍓嶅鐞嗘妧鏈紝騫挎硾鍦板簲鐢ㄤ簬鐜姹℃煋鐗┿�佹按浣撶瓑鐥曢噺鐗╄川鐨勬嫻媅4]銆傚埄鐢⊿PEM綰ょ淮澶磋杽鑶滃鍖栧悎鐗╃殑鍚擱檮銆佸瘜闆嗭紝鍐嶄笌姘旂浉鑹茶氨璐ㄨ氨鑱旂敤錛屽彲楂樿揪10-9鐨勬嫻嬬駭鍒�備簯鍗楀ぇ瀛﹁浼犲潳銆佽帿鏄庡拰寮犲厠鍕ゅ埄鐢ㄥ浐鐩稿井钀冨彇鎶�鏈?姘旂浉鑹茶氨璐ㄨ氨娉曪紙SPEM-GC/MS錛夛紝嫻嬪畾浜嗗弬涓庡湡澹ゆ姂鐪熻弻浣滅敤鐨勫湡澹ゆ尌鍙戞�ф垚鍒嗗拰鍦熷￥緇嗚弻鎸ュ彂鎬т唬璋㈢墿[5]銆?/span>
鍥涳紝闆墮《絀烘妧鏈浂欏剁┖鎶�鏈槸涓�縐嶅湪鍏ㄥ瘑闂�侀珮鍘嬬姸鎬佷笅錛屽皢鍥轟綋搴熺墿涓殑鎸ュ彂鎬ф湁鏈虹墿鎻愬彇鑷蟲蹈娉℃恫鍚庯紝鍐嶉噰鐢ㄩ《絀烘垨鍚規(guī)壂鐨勬柟娉曞皢嫻稿嚭娑蹭腑鐨勬尌鍙戞�ф湁鏈虹墿榪涜嫻嬪畾鐨勪竴縐嶆妧鏈�?/span>
浜旓紝闈欐�侀《絀烘硶銆傜敱浜庢尌鍙戞�ф湁鏈虹墿鐨勬哺鐐硅緝浣庯紝閫氳繃鍔犵儹鏍峰搧鐡朵腑鏍峰搧錛屽疄鐜版薄鏌撶墿鍦ㄦ皵/娑詫紙鍥猴級涓ょ浉闂寸殑鍚堢悊鍒嗛厤錛屽茍淇濇寔姘旀恫騫寵 錛屽湪姘旀恫騫寵 鍚庢娊鍙栧瓨鍦ㄤ笂闈㈢殑鎴愬垎錛屼箣鍚庢敞鍏ュ埌姘旂浉鑹茶氨鎴栨皵鐩歌壊璋辮川璋辮仈鐢ㄤ華榪涜鍒嗘瀽鐨勮繃紼嬨�傚鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氾紝闈欐�侀《絀烘硶涓庡惞鎵崟闆嗘硶鐩告瘮錛屾搷浣滅畝鍗曪紝鎴愭湰闈炲父浣庯紝鏂逛究鑷姩鍖栵紝浣嗘槸涔熷瓨鍦ㄧ伒鏁忓害杈冧綆錛屾祴瀹氭晥鏋滀笉浣砙6]銆?/span>
鎬葷粨
緇間笂鎵�榪幫紝鐮旂┒鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氭柟娉曪紝淇濊瘉嫻嬭瘯鐨勭瀛︽�т笌鏈夋晥鎬ч潪甯擱噸瑕侊紝鏈夊姪浜庤揪鍒扮悊鎯崇殑嫻嬪畾鏁堟灉錛屼繚璇佸湡澹ゆ尌鍙戞�ф湁鏈虹墿嫻嬪畾鏁堟灉錛屾柟渚胯繘琛屾繁鍏ョ殑鐮旂┒錛屼繚璇佸伐浣滄椿鍔ㄧ殑欏哄埄瀹炴柦錛岀‘淇濆伐浣滄晥鐜囦笌璐ㄩ噺銆傛�昏�岃█涔嬶紝鐮旂┒鍦熷￥鎸ュ彂鎬ф湁鏈虹墿姹℃煋鐨勭壒鎬с�佺壒寰佷笌嫻嬪畾鏂規(guī)硶鍏鋒湁閲嶈鐨勬剰涔変笌浠峰�鹼紝鏈夊姪浜庝繚璇佸伐浣滄晥鐜囦笌璐ㄩ噺銆?/span>
鍓嶈█
嫻嬪畾鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勭浉鍏沖唴瀹癸紝瀵規(guī)尌鍙戞�ф湁鏈虹墿榪涜姒傝堪闈炲父閲嶈錛屽彲浠ユ竻妤氬湡澹ゆ尌鍙戞�ф湁鏈虹墿姹℃煋鐨勭壒寰佷笌鐗圭偣錛岄�夋嫨鎭板綋鐨勫湡澹ゆ尌鍙戞�ф湁鏈虹墿嫻嬪畾鏂規(guī)硶錛岄�氳繃瀹為獙鎵嬫錛岃繘琛屽疄楠屽垎鏋愶紝瀵圭粨鏋滆繘琛屾繁鍏ョ殑璁ㄨ鎺㈢┒錛屼繚璇佸伐浣滅殑欏哄埄瀹炴柦銆傜敱姝ゅ彲瑙侊紝鐮旂┒鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氬叿鏈夐噸瑕佺殑鎰忎箟涓庝環(huán)鍊鹼紝鏈夊姪浜庡彂鎸ラ噸瑕佺殑浣滅敤錛屾帉鎻℃湁鏁堢殑鍦熷￥鎸ュ彂鎬ф湁鏈虹墿嫻嬪畾鏂規(guī)硶錛屼繚璇佹祴瀹氱殑縐戝鎬т笌鍚堢悊鎬с�?/span>
涓�銆佹尌鍙戞�ф湁鏈虹墿鐨勬榪?/span>
闅忕潃縐戞妧鐨勫揩閫熷彂灞曪紝鐜頒唬鍐滀笟鍜屽寲宸ヤ紒涓氭帓鏀句簡澶ч噺搴熸按銆佸簾姘斻�佸簾鐗╋紝鍦ㄥ湡澹ゃ�佺┖姘斾互鍙婄敓鐗╃瓑浠嬭川鐨勮漿鍖栦笅錛岄暱鏈熷瓨鍦ㄤ簬鍦熷￥浠ュ強姘翠綋涓紝褰㈡垚鍥哄畾姹℃煋[1]銆傛綾葷墿璐ㄤ笌浜洪暱鏈熸帴瑙︼紝鏋佹槗閫犳垚浜轟綋鎱㈡�т腑姣掞紝鐢氳嚦浼?xì)璇卞彂鐧岀棁锛屽錆h綾婚�犳垚杈冨ぇ鐨勫獎鍝嶏紝鐩存帴褰卞搷鍒扮敓孌栦笌涓灑紲炵粡緋葷粺錛屽湪涓ラ噸鎯呭喌涓嬶紝鐢氳嚦浼?xì)瀵艰嚧錆h綾繪浜★紝鍚屾椂錛屼篃浼?xì)瀵圭幆澧冨甫鏉ヤ弗閲嶇殑鍗卞疅雬傞櫎姝や箣澶栵紝搴熺墿緇忚繃闆ㄦ按鐨勫啿鍒鳳紝浼?xì)瀵瑰湴琛ㄦ按浠ュ強鍦颁笅姘撮�犳垚姹℃煋錛屽鑷翠弗閲嶇殑鍚庢灉銆傚熀浜庢錛岀爺絀跺湡澹や腑鎸ュ彂鎬ф湁鏈虹墿媯�嫻嬮潪甯擱噸瑕侊紝涓嬮潰瀵規(guī)尌鍙戞�ф湁鏈虹墿榪涜璇︾粏鐨勬榪般�傜幇闃舵錛屾尌鍙戞�ф湁鏈虹墿鐨勬潵婧愪富瑕佸垎涓轟互涓嬩袱縐嶏紝浜轟負(fù)鎺掓斁鐨勪笌鑷劧鎺掓斁鐨勩�備漢涓烘帓鏀劇殑涓昏鍖呮嫭鍖栧伐鐢熶駭浜х敓鐨勬苯杞﹀熬姘斻�傛尌鍙戞�ф湁鏈虹墿瀵逛漢浣撳拰鐜鏈夌潃杈冨ぇ鐨勫嵄瀹籌紝鍥犳錛屼漢綾誨湪闀挎湡鍙楀埌鎸ュ彂鎬ф湁鏈虹墿鍗卞鏃訛紝鏋佹槗浜х敓鐥呭彉錛屽獎鍝嶄漢綾昏韓浣撳仴搴楓�傛尌鍙戞�ф湁鏈虹墿涓昏鏉ヨ嚜瀹ゅ錛屽澶栦富瑕佹槸鐢變簬鐕冩枡浠ュ強宸ヤ笟搴熸皵銆佹苯杞﹀熬姘旂瓑璇卞彂鐨勩�傚嚭鐜版尌鍙戞�ф湁鏈虹墿鐨勫師鍥犱富瑕佹槸澶╃劧姘旂噧鐑с�佸惛鐑熴�佺児璋冧互鍙婇噰鏆栥�傚湪瀹ゅ唴瑁呴グ榪囩▼涓紝鎸ュ彂鎬ф湁鏈虹墿鍒欎富瑕佹潵鑷簬娑傛枡浠ュ強娌規(guī)紗銆傛尌鍙戞�ф湁鏈虹墿浣滀負(fù)涓�縐嶆薄鏌撴簮錛屼富瑕佸垎涓轟互涓嬪嚑縐嶏細(xì)涓�錛屾湁鏈烘憾娑層�傛湁鏈烘憾娑蹭富瑕佹槸鐢辨湁鏈虹墿緇勬垚鐨勬憾鍓傦紝鍏朵腑鐨勬樉钁椾唬琛ㄥ氨鏄寲濡嗗搧銆佹補婕嗐�佺矘鍚堝墏浠ュ強鍚按娑傛枡絳夛紱浜岋紝寤虹瓚鏉愭枡錛屽緩絳戞潗鏂欐槸鎸囧緩絳戝伐紼嬩腑浣跨敤鐨勬尌鍙戞皵鍛蟲潗鏂欙紝涓昏鍖呮嫭浜洪�犳澘鏉愩�佹秱鏂欍�佹場娌殧鐑潗鏂欑瓑[2]錛涗笁錛岀氦緇存潗鏂欙紝綰ょ淮鏉愭枡鏄寚鍚堟垚綰ょ淮鍒舵垚鐨勬潗鏂欎互鍙婂ぉ鐒剁氦緇村埗鎴愮殑鏉愭枡錛屼富瑕佹寚鍦版銆佸寲綰ょ獥甯樹互鍙婃寕姣瓑錛涘洓錛屽澶栧伐涓氭皵浣擄紝瀹ゅ宸ヤ笟姘斾綋鑼冨洿騫挎硾錛屼富瑕佹槸鎸囧伐涓氱敓浜т互鍙婃満姊版暎鍙戝嚭鏉ョ殑姘斾綋銆佺敓浜ц繃紼嬪埗閫犵殑浠ュ強姹借濺灝炬皵絳夈�?/span>
浜屻�佸湡澹ゆ尌鍙戞�ф湁鏈虹墿姹℃煋鐨勭壒鎬т笌鐗瑰緛
鎸ュ彂鎬ф湁鏈虹墿浣滀負(fù)涓�縐嶆薄鏌撴簮錛屽叿鏈夋樉钁楃殑姹℃煋鐗規(guī)�э紝鍏舵薄鏌撶壒鎬т笌鐗瑰緛涓昏浣撶幇鍦ㄤ互涓嬩袱涓柟闈紝鍒嗗埆鏄尌鍙戞�ф湁鏈虹墿鐨勬薄鏌撶壒鎬т互鍙婂湪鍦熷￥涓殑鍒嗗竷榪佺Щ銆?/span>
鎸ュ彂鎬ф湁鏈虹墿鐨勬薄鏌撶壒鎬т富瑕佸寘鎷互涓嬪洓涓柟闈㈠唴瀹癸細(xì)涓�錛屾尌鍙戞�э紝鎸ュ彂鎬ф湁鏈虹墿鐨勬樉钁楃壒寰佸氨鏄叿鏈夎緝寮虹殑鎸ュ彂鎬э紝涓�鏃︽弧瓚沖帇鍔涗笌娓╁害鏉′歡錛屽氨鑳藉浠庡湡澹や腑鎸ュ彂錛屽茍榪涘叆澶ф皵錛岄�犳垚涓ラ噸鐨勫嵄瀹籌紝鍏鋒湁杈冨己鐨勬薄鏌撴�э紱浜岋紝闅愯斀鎬э紝鍦熷￥涓殑鎸ュ彂鎬ф湁鏈虹墿鍏鋒湁杈冨己鐨勯殣钄芥�э紝甯稿父浼?xì)闅愯棌鍦ㄥ湡澹や腑锛寴q樹細(xì)闅愯棌鍦ㄦ皵浣撱�佹恫浣撱�佸浐浣撶瓑鐗╄川涓紝鍏鋒湁闈炲父澶х殑闅愯棌鎬э紱涓夛紝鎸佷箙鎬э紝鎸ュ彂鎬ф湁鏈虹墿涓�鏃﹁繘鍏ュ埌澶ф皵涓紝鏄壒鍒毦浠ユ竻闄ょ殑錛岄殢鐫�鎸ュ彂閲忕殑鎻愬崌錛屾祿搴︾殑涓嶆柇鎻愰珮錛屽叾緇撴灉鏄祿搴︿細(xì)瓚呰繃浜轟綋鐨勫彲鎵垮彈鑼冨洿錛屽浜轟綋閫犳垚涓嶅彲鎸藉洖鐨勪激瀹籌紝鍗卞浜轟綋鐨勮韓浣撳仴搴鳳紱鍥涳紝姣掑鎬э紝鎸ュ彂鎬ф湁鏈虹墿澶у鏄叿鏈夋瘨鎬х殑錛屼笖姣掓�ц緝寮猴紝灝ゅ叾鏄湁姣掓�х殑姹℃煋鐗╂尌鍙戝埌澶ф皵涓紝浼?xì)迮炴垚鍏夊寲瀛︾儫闆惧Q屽澶ф皵鐜閫犳垚涓ラ噸鐨勫獎鍝嶃�?/span>
鎸ュ彂鎬ф湁鏈虹墿鍦ㄥ湡澹や腑鐨勮縼縐葷壒鎬э紝浠ユ皵鎬佷互鍙婃恫鎬佷袱縐嶆柟寮忓嚭鐜幫紝鍐嶈�咃紝鎸ュ彂鎬ф湁鏈虹墿鍏鋒湁寮虹儓鐨勬尌鍙戞�э紝瀹規(guī)槗榪涘叆鍒頒漢綾葷敓媧葷殑澶ф皵涓紝涔熷鏄撹繘鍏ュ埌姘翠腑錛屾瀬鏄撳浜虹被鐢熸椿閫犳垚濞佽儊銆傚悓鏃訛紝鎸ュ彂鎬ф湁鏈虹墿涔熷叿澶囪縼縐繪�э紝淇濊瘉鍏跺緇堝浜庡姩鎬佸彉鍖栬繃紼嬩腑錛屼笖鏄笉鏂彉鍖栫殑錛屽洜鑰岋紝鎸ュ彂涔熸槸涓�縐嶈縼縐葷殑鏂瑰紡錛屽叿鏈夎縼縐葷壒鎬с�?/span>
涓夈�佸湡澹や腑鎸ュ彂鎬ф湁鏈虹墿嫻嬪畾鏂規(guī)硶
鍦ㄥ湡澹ゆ尌鍙戞�ф湁鏈虹墿嫻嬪畾榪囩▼涓紝鎺屾彙縐戝鐨勬祴瀹氭柟娉曘�佷繚璇佹祴瀹氱殑鏈夋晥鎬ч潪甯擱噸瑕侊紝鍥犳錛屾帉鎻″湡澹ゆ尌鍙戞�ф湁鏈虹墿嫻嬪畾鏂規(guī)硶鍏鋒湁閲嶈鐨勬剰涔夈�傚湡澹や腑鎸ュ彂鎬ф湁鏈虹墿嫻嬪畾鏂規(guī)硶涓昏鍖呮嫭浠ヤ笅鍑犵錛?/span>
涓�錛屼究鎼哄紡姘旂浉鑹茶氨浠硶[2]銆備究鎼哄紡姘旂浉鑹茶氨浠槸涓�嬈捐秴鐏墊晱銆佷綆鍔熻�楀拰蹇�熸嫻嬫尌鍙戞�ф湁鏈虹墿鐨勪究鎼哄紡姘旂浉鑹茶氨浠紝灝ゅ叾閫傜敤浜庢嫻嬫尌鍙戞�ф湁鏈虹墿濡傝嫰銆佺敳鑻�佷箼鑻�侀偦錛岄棿錛屽浜岀敳鑻瓑鑻郴鐗╋紝鐗圭偣浣撶Н灝忋�侀噸閲忚交錛屽叿鏈夎秴楂樼伒鏁忓害鐨勫厜紱誨瓙鍖栨嫻嬪櫒銆備富瑕佹槸瀵圭┖姘斿唴鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氥�?/span>
浜岋紝鍚規(guī)壂鎹曢泦娉曘�傚惞鎵崟闆嗘妧鏈�傜敤浜庝粠娑蹭綋鎴栧浐浣撴牱鍝佷腑钀冨彇娌哥偣浣庝簬200鈩冦�佹憾瑙ｅ害灝忎簬2%鐨勬尌鍙戞�ф垨鍗婃尌鍙戞�ф湁鏈虹墿錛屾槸鐜鐩戞祴涓噸瑕佺殑鏂規(guī)硶銆傚湪娑蹭綋鎴栧浐浣撲腑鐨勬尌鍙戞�ф湁鏈虹墿錛岀敤姘皵銆佹唉姘旀垨鍏跺畠鎯版�ф皵浣撳皢琚祴鐗╀粠鏍峰搧涓娊鎻愬嚭鏉ャ�傚惞鎵崟闆嗘妧鏈嬌姘斾綋榪炵畫閫氳繃鏍峰搧錛屽皢鍏朵腑鐨勬尌鍙戠粍鍒嗚悆鍙栧悗鍦ㄥ惛闄勫墏鎴栧喎闃變腑鎹曢泦錛屽啀榪涜鍒嗘瀽嫻嬪畾錛屾槸涓�縐嶉潪騫寵 鎬佺殑榪炵畫钀冨彇銆傚惞鎵崟闆嗘硶瀵規(guī)牱鍝佺殑鍓嶅鐞嗘棤闇�浣跨敤鏈夋満婧跺墏錛屽鐜涓嶉�犳垚浜屾姹℃煋錛岃�屼笖鍏鋒湁鍙栨牱閲忓皯銆佸瘜闆嗘晥鐜囬珮銆?/span>
鍦ㄥ惞鎵崟闆嗘硶搴旂敤榪囩▼涓紝褰卞搷嫻嬭瘯緇撴灉鐨勫師鍥犱富瑕佹湁涓や釜鏂歸潰錛屼竴鏄惞鎵椂闂寸殑閫夋嫨錛屽惞鎵椂闂存槸褰卞搷鐏墊晱搴︿互鍙婂洖鏀剁巼鐨勯噸瑕佸洜绱狅紝鍦ㄥ惞鎵椂闂磋緝闀跨殑鎯呭喌涓嬶紝浼?xì)鍚硅劚鍚搁檮鍓傚Q屽獎鍝嶆祴瀹氭晥鏋溿�傚湪鍚規(guī)壂鏃墮棿鍋忕煭鐨勬儏鍐典笅錛屽垎鏋愮墿鎸ュ彂涓嶅厖鍒嗭紝涔熶細(xì)褰卞搷嫻嬪畾鏁堟灉銆備簩鏄敳閱囦笌姘寸殑騫叉壈銆傚湪鍚規(guī)壂鎹曢泦娉曞簲鐢ㄨ繃紼嬩腑錛岀敳閱囦笌姘翠細(xì)瀵規(guī)祴瀹氭晥鏋滈�犳垚褰卞搷錛屽共鎵版嫻嬪櫒淇″彿錛屽獎鍝嶆嫻嬬殑鍑嗙‘搴3]銆?/span>
涓夛紝鍥虹浉寰悆鍙栵紙SPME錛夊浐鐩稿井钀冨彇鎶�鏈紙SPEM錛夋槸榪戝勾鏉ュ彂灞曡搗鏉ヤ竴縐嶆棤闇�婧跺墏錛岄泦钀冨彇銆佹祿緙╁拰榪涙牱涓轟竴浣撶殑鏍峰搧鍓嶅鐞嗘妧鏈紝騫挎硾鍦板簲鐢ㄤ簬鐜姹℃煋鐗┿�佹按浣撶瓑鐥曢噺鐗╄川鐨勬嫻媅4]銆傚埄鐢⊿PEM綰ょ淮澶磋杽鑶滃鍖栧悎鐗╃殑鍚擱檮銆佸瘜闆嗭紝鍐嶄笌姘旂浉鑹茶氨璐ㄨ氨鑱旂敤錛屽彲楂樿揪10-9鐨勬嫻嬬駭鍒�備簯鍗楀ぇ瀛﹁浼犲潳銆佽帿鏄庡拰寮犲厠鍕ゅ埄鐢ㄥ浐鐩稿井钀冨彇鎶�鏈?姘旂浉鑹茶氨璐ㄨ氨娉曪紙SPEM-GC/MS錛夛紝嫻嬪畾浜嗗弬涓庡湡澹ゆ姂鐪熻弻浣滅敤鐨勫湡澹ゆ尌鍙戞�ф垚鍒嗗拰鍦熷￥緇嗚弻鎸ュ彂鎬т唬璋㈢墿[5]銆?/span>
鍥涳紝闆墮《絀烘妧鏈浂欏剁┖鎶�鏈槸涓�縐嶅湪鍏ㄥ瘑闂�侀珮鍘嬬姸鎬佷笅錛屽皢鍥轟綋搴熺墿涓殑鎸ュ彂鎬ф湁鏈虹墿鎻愬彇鑷蟲蹈娉℃恫鍚庯紝鍐嶉噰鐢ㄩ《絀烘垨鍚規(guī)壂鐨勬柟娉曞皢嫻稿嚭娑蹭腑鐨勬尌鍙戞�ф湁鏈虹墿榪涜嫻嬪畾鐨勪竴縐嶆妧鏈�?/span>
浜旓紝闈欐�侀《絀烘硶銆傜敱浜庢尌鍙戞�ф湁鏈虹墿鐨勬哺鐐硅緝浣庯紝閫氳繃鍔犵儹鏍峰搧鐡朵腑鏍峰搧錛屽疄鐜版薄鏌撶墿鍦ㄦ皵/娑詫紙鍥猴級涓ょ浉闂寸殑鍚堢悊鍒嗛厤錛屽茍淇濇寔姘旀恫騫寵 錛屽湪姘旀恫騫寵 鍚庢娊鍙栧瓨鍦ㄤ笂闈㈢殑鎴愬垎錛屼箣鍚庢敞鍏ュ埌姘旂浉鑹茶氨鎴栨皵鐩歌壊璋辮川璋辮仈鐢ㄤ華榪涜鍒嗘瀽鐨勮繃紼嬨�傚鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氾紝闈欐�侀《絀烘硶涓庡惞鎵崟闆嗘硶鐩告瘮錛屾搷浣滅畝鍗曪紝鎴愭湰闈炲父浣庯紝鏂逛究鑷姩鍖栵紝浣嗘槸涔熷瓨鍦ㄧ伒鏁忓害杈冧綆錛屾祴瀹氭晥鏋滀笉浣砙6]銆?/span>
鎬葷粨
緇間笂鎵�榪幫紝鐮旂┒鍦熷￥鎸ュ彂鎬ф湁鏈虹墿鐨勬祴瀹氭柟娉曪紝淇濊瘉嫻嬭瘯鐨勭瀛︽�т笌鏈夋晥鎬ч潪甯擱噸瑕侊紝鏈夊姪浜庤揪鍒扮悊鎯崇殑嫻嬪畾鏁堟灉錛屼繚璇佸湡澹ゆ尌鍙戞�ф湁鏈虹墿嫻嬪畾鏁堟灉錛屾柟渚胯繘琛屾繁鍏ョ殑鐮旂┒錛屼繚璇佸伐浣滄椿鍔ㄧ殑欏哄埄瀹炴柦錛岀‘淇濆伐浣滄晥鐜囦笌璐ㄩ噺銆傛�昏�岃█涔嬶紝鐮旂┒鍦熷￥鎸ュ彂鎬ф湁鏈虹墿姹℃煋鐨勭壒鎬с�佺壒寰佷笌嫻嬪畾鏂規(guī)硶鍏鋒湁閲嶈鐨勬剰涔変笌浠峰�鹼紝鏈夊姪浜庝繚璇佸伐浣滄晥鐜囦笌璐ㄩ噺銆?/span>
鐩稿叧鏍囩
鐩稿叧鏂伴椈
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鍏徃閭錛?/p>
鍏徃鍦板潃錛氫節(jié)榫欏潯鍖哄崕宀╅晣澹規(guī)湰縐戝伐鍩?/p>
